CiteULike: Chelation-Assisted, Copper(II)-Acetate-Accelerated Azide?Alkyne Cycloaddition
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CiteULike: Chelation-Assisted, Copper(II)-Acetate-Accelerated Azide?Alkyne Cycloaddition
Gui-Chao Kuang, Heather A. Michaels, J. Tyler Simmons, Ronald J. Clark, Lei Zhu. The Journal of Organic Chemistry, Vol. 75, No. 19. (1 October 2010), pp. 6540-6548. We described in a previous communication a variant of the popular CuI-catalyzed azide?alkyne cycloaddition (AAC) process where 5 mol % of Cu(OAc)2 in the absence of any added reducing agent is sufficient to enable the reaction. 2-Picolylazide (1) and 2-azidomethylquinoline (2) were found to be by far the most reactive carbon azide su
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